Hi,
Did my second attempt today, and it went much smoother this time.
As you can see in the picture,
To the left you have the "waterlayer" after extraction with NaOH 25%, and to the right you have the amphetamine-oil, freebase, a-oil, what ever you want to call it.
In the waterlyer flask you can see about 5ml of A-oil that I could not extract, I mixed the waterlayer with IPA and extracted the ipa layer, unfortunetly my home made distiller did not work, too many joints to grease and to much hustle, in my opinion it's not worth the extra effort for a few extra ml.
I will need to invest in a rotovap later.
The amphetamine-oil was cleaned three times through buchner funnel and clean filters each time.
Let me know what you think.
Best Regards