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It would affect the yield, sodium borohydride creates an exothermic reaction and that's how it works.
You could try to keep it steady at around 60c while you add the p2np but it could be quite hard.
You could try to keep it steady at around 60c while you add the p2np but it could be quite hard.
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I was thinking maybe dissolving the starting material in IPA and slowly drip it into the reaction vessel using a SEP funnel. You recon that would affect it negatively in any way?