Al/Hg aracılığıyla P2NP'den amfetamin sentezi (video)
- Thread starter HIGGS BOSSON
- Start date
so i have an oily residue product,what is a good way to crystalize it?
Thank you for the previous responses.
The chemist has carried out their first (successful?) reaction and, as a result, has further questions.
The test subject, who evaluated the final product, compared it to the one commonly available on the street (according to police reports found online, its purity is usually around 10-20%).
I’d like to know whether the test subject had overly high expectations of the product, or if the inexperienced chemist might have made several mistakes during the process?
What can realistically be expected from the final product, and could further experiments significantly improve its quality?
The errors that, according to the chemist, may have affected the final product include:
• Completely skipping extraction with DCM (the chemist was prepared for it but lacked sufficient theoretical knowledge).
• Drying the product for too short a time and at too high a temperature.
Could this affect the product’s quality?
Does extraction with DCM involve adding DCM to the free base and collecting the appropriate layer? If so, are the layers clearly distinguishable, and which one (top/bottom) contains the product?
Could @G.Patton @William D. provide their input on this?
Thank you!
The chemist has carried out their first (successful?) reaction and, as a result, has further questions.
The test subject, who evaluated the final product, compared it to the one commonly available on the street (according to police reports found online, its purity is usually around 10-20%).
I’d like to know whether the test subject had overly high expectations of the product, or if the inexperienced chemist might have made several mistakes during the process?
What can realistically be expected from the final product, and could further experiments significantly improve its quality?
The errors that, according to the chemist, may have affected the final product include:
• Completely skipping extraction with DCM (the chemist was prepared for it but lacked sufficient theoretical knowledge).
• Drying the product for too short a time and at too high a temperature.
Could this affect the product’s quality?
Does extraction with DCM involve adding DCM to the free base and collecting the appropriate layer? If so, are the layers clearly distinguishable, and which one (top/bottom) contains the product?
Could @G.Patton @William D. provide their input on this?
Thank you!
- By G.Patton
Hello.
It is quite subjective, has he checked its melting point? Isomer ratio also play role in the product activity. In addition, there is direct dependence between its purity and potency.
It's hard to estimate its quality in accordance with your description. You should check its purity in laboratory (such as EnergyControl or so) and then try to find a problem. Is your product absolutely white?
this step is quite important in order to increase the reaction yield and get rid of Hg salts in final product.
It also can influence on the product quality in case of air exposure during its strong heating.
Yes, he has to add DCM to the reaction mixture stir it well and then separate layers. DCM layer is clearly be determinated by its transparency and smell.
By the way, will you sell your product here?
It is quite subjective, has he checked its melting point? Isomer ratio also play role in the product activity. In addition, there is direct dependence between its purity and potency.
It's hard to estimate its quality in accordance with your description. You should check its purity in laboratory (such as EnergyControl or so) and then try to find a problem. Is your product absolutely white?
this step is quite important in order to increase the reaction yield and get rid of Hg salts in final product.
It also can influence on the product quality in case of air exposure during its strong heating.
Yes, he has to add DCM to the reaction mixture stir it well and then separate layers. DCM layer is clearly be determinated by its transparency and smell.
By the way, will you sell your product here?