Kannabidiolün (CBD) Psikoaktif Kannabinoidlere İzomerizasyonu

kitboy

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GqYXjsEBI7


CBD pişiriyordum ve yanlışlıkla karışıma NAoh ekledim, sanırım izomerizasyon durdu. 2 katman oluştu, biri bana ne oluştuğunu söyleyebilir mi? THC özütü çıkarmak için iyi bir yol mu?

Metanol ve HCL kullanıyorum
 

G.Patton

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Merhaba, NaOH'ı hangi aşamada eklediniz?

Cevap HPLC analizi ile verilebilir.
 
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kitboy

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2 saatlik izomerizasyondan sonra bir yağ oluştu ancak hoş olmayan bir kokusu var ve onu nasıl saflaştıracağımı bilmiyorum.
 

kitboy

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Naoh eklerken iki faz birbirinden ayrıldı ve sanırım reaksiyon durdu. Birçok şekilde yıkamayı denedim ama o kötü kokudan kurtulamıyorum.
 

cvvvxa

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Bazlar cbd'yi (thc dönüşmez) bazı kinon türevlerine dönüştürür. sanırım thc'den ayırmak için farklı çözücüler kullanılabilir ama hangisinin hangi literatürde tanımlandığını hatırlayamıyorum ayrıca yeşil olduğu için (sanırım) bazı bitki safsızlıkları da oksitlenebilir
 

kitboy

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Asetik asit mi yoksa hidroklorik asit mi daha iyidir? Temizlemek veya saf cbd loas'ı metanolden çıkarmak için yaptığım iğrenç bir koku ile bırakılmış bir yağım var
 

cvvvxa

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oda sıcaklığında toluen ve p-toluensülfonik asit neredeyse saf delta 9 için kullanılabilir ve ısı ile diğer çözücüler delta 8 ile sonuçlanır
 

cvvvxa

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tolueni çıkarmak zor olabilir, ancak 44 saat (48 saat biraz daha fazla dönüşümle sonuçlanacaktır, ancak yaklaşık% 10 delta8) karıştırılmış% 10 ptsa ve onu çözmek için yeterli toluen, daha sonra çalışma
 

kitboy

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Aside karşı koymak için NAOH ile doyurulmuş su eklediğinizde, hepsini elimine edemiyorum ve çok fazla su eklersem üst faz siyaha dönüyor. Ekstraksiyonu nasıl yapabilirim? Asit kokusunu nasıl yok edebilirim? Damıtılmış su ile temizlemeyi denedim ama işe yaramadı.

Bu konuda yardıma ihtiyacım var lütfen

THC'yi hangi PH'da bırakmalıyım? THC'yi saflaştırmak için bütan veya toluen kullanabilir miyim?
 

WillD

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Katalitik miktarlarda asit kullanan yöntemler kendilerini bu konudan daha iyi kanıtlamıştır. DCM içinde %10 mol pTSA (delta-8) veya etanol içinde %0,05 HCl (delta-9) ile
 

Dr. MMX

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Ethyl aclohol'den farklı bir alkol kullanılabilir mi? belki ipa yerine?
hcl kullanılabilir mi?
 
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Irving Langmuir

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Reaktifleriniz çözünebilir olduğu sürece bence de öyle. HCl bir asit katalizörü olarak kullanılabilir.
 

WillD

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The change of solvent and the amount of acid greatly changes the composition of the result
 

kitboy

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I think it is better to use methanol
 

Kvadprime

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I love vape with TGK ... I think I can do:

1. We carry out isomerization in ethanol with acetic acid for 12-24h.
2. After - we evolve all ethanol and acetic acid
3. Pour the resin with a mixture of glycerol and propylene glycol, dissolving gravs completely
4. Pour into a comfortable jar and smoke

The issue of health safety - alcohol and acetic acid should clearly not be synthetic - only food (We make THC from the CBD using trembling and sugar, aahahhaha)

Experienced isomerization specialists - what do you think? Is it worth a try?
 

Kvadprime

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I love vape with TGK ... I think I can do:

1. Start reaction in ethanol with acetic acid for 12-24h.
2. After - we evaporate all the ethanol and acetic acid
3. Pour the resin with a mixture of glycerol and propylene glycol, dissolving gravs completely
4. Pour into a comfortable jar and smoke

The issue of health safety - alcohol and acetic acid should clearly not be synthetic - only food (We make THC from the CBD using trembling and sugar, aahahhaha)

Experienced isomerization specialists - what do you think? Is it worth a try?
 

WillD

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You do not have to evaporate it. You can dilute with water and separate the oil if you use ethanol.
 
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Kvadprime

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Hmmm... Of course!
And question

If I use AcOH in concentration about of 70-80%, It get to start isomerisation?

Now.... I can't get or make 100% acetic acid((
 

WillD

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Then you need 7.5 (70%) - 6.5 (80%) mL of acetic acid soln. per ~100mL of ethanol (approximately).
Excess ethanol is necessary for the reaction to go well.
The resulting solution will take 5-10 g of cbd powder, nothing more.
Heat up to 70*C and boil at least 2 hours.
Dilute with water and collect the resulting oil.
You can write us about your results after.
 

Kvadprime

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Ok! I try to do it, thx!!

But 5g cbd in my town i cant get with good price for first try

I try with 1g cbd in 10ml ethanol with ~1ml AcOH

Thx!!!!!!!
 

WillD

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The reaction time can be a little longer than we wrote before. You need to examine to choose the best time if you do not have the opportunity to make an analyst.
 

Rabidreject

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I have wanted to do this for ages but have been holding off as I don’t have p-tsa, however, if d9 is generally done with a catalytic amount of HCl, that would be MUCH easier.
Is it literally a case of chucking it all in, letting it react for ages at RT (12-24h I think I heard), quenching, extracting?

Seeing as THC is by far the drug I use the most, it would make sense for edibles or whatever. Doubt I would want to vape it though. Never was a huge fan of vaping distillate as it just screws my tolerance.

It looks pretty easy though
 

Kvadprime

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Yes, it looks simple. That's why I want to try it!.. I'll write when I do it, there will be another report
 

WillD

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If you use HCl for conversion, then heating is required.
 
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