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- Nov 5, 2022
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I did it like this a long time ago:
1 Liter of Ipa (isopropyl alcohol) 99% laboratory grade (the "drugstore" grade does not work)
1 Liter of 99% acetone ("drugstore" grade does not work and less than Mercadona)
1 glass of 1 liter
1 hot plate (but since not everyone has it, a double boiler is an option)
1 laboratory thermometer
That's all.
For each gram of Mdma we need 3.50 ml of ipa (measurements are very important!)
We put the ipa in a beaker and also a thermometer touching the ipa
We heat the ipa to 55 degrees (do not exceed 60 degrees)
Once we have that temperature, we put the Mdma and it will dissolve
Cover the glass with a piece of paper and leave it at room temperature for 4 hours.
After those 4 hours it should be in the fridge for a day
the day after freezing for another day and the crystals are already forming
First batch:
Pour the dirty ipa into another glass and put it back in the freezer.
in the beaker with the crystals we add acetone (half ipa) the beaker is so cold that the crystals dissolve and the acetone blocks it.
approximately in an hour that same acetone we overturned it in the dirty ipa glass
We let the crystals dry for a day.
Why do we add acetone to the ipa? Because there are still crystals, but we need acetone, otherwise the crystals will not form.
With the discarded acetone we add it to the dirty ipa glass from the freezer. Without the acetone, the second batch of crystals won't form!
these crystals will take longer to form, leave them in the freezer for a few days
We took out the glass and threw away the dirty ipa.
We add acetone so that the crystals do not dissolve. When the glass is at room temperature, we throw away the acetone and let the crystals dry
1 Liter of Ipa (isopropyl alcohol) 99% laboratory grade (the "drugstore" grade does not work)
1 Liter of 99% acetone ("drugstore" grade does not work and less than Mercadona)
1 glass of 1 liter
1 hot plate (but since not everyone has it, a double boiler is an option)
1 laboratory thermometer
That's all.
For each gram of Mdma we need 3.50 ml of ipa (measurements are very important!)
We put the ipa in a beaker and also a thermometer touching the ipa
We heat the ipa to 55 degrees (do not exceed 60 degrees)
Once we have that temperature, we put the Mdma and it will dissolve
Cover the glass with a piece of paper and leave it at room temperature for 4 hours.
After those 4 hours it should be in the fridge for a day
the day after freezing for another day and the crystals are already forming
First batch:
Pour the dirty ipa into another glass and put it back in the freezer.
in the beaker with the crystals we add acetone (half ipa) the beaker is so cold that the crystals dissolve and the acetone blocks it.
approximately in an hour that same acetone we overturned it in the dirty ipa glass
We let the crystals dry for a day.
Why do we add acetone to the ipa? Because there are still crystals, but we need acetone, otherwise the crystals will not form.
With the discarded acetone we add it to the dirty ipa glass from the freezer. Without the acetone, the second batch of crystals won't form!
these crystals will take longer to form, leave them in the freezer for a few days
We took out the glass and threw away the dirty ipa.
We add acetone so that the crystals do not dissolve. When the glass is at room temperature, we throw away the acetone and let the crystals dry
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- Joined
- Jan 6, 2023
- Messages
- 280
- Reaction score
- 112
- Points
- 43
As I understand, MDMA solubility in boiling IPA is around 1.4 ml of IPA per 1 gr of chloride.
May be, you can specify what is MDMA solubility in IPA at RT and frozen IPA?
May be, you can specify what is MDMA solubility in IPA at RT and frozen IPA?
- Joined
- Jan 6, 2023
- Messages
- 280
- Reaction score
- 112
- Points
- 43
I empirically found interesting fact. Solubility in IPA depends on purity.
I had two batches, one after ABE, pure white, another one brownish after crystallization in water.
Both batches were solved by weight in IPA from the same bottle under T=65C.
Chloride weight - 70 gr
IPA weight - 193 gr
First flask dissolved completely.
Second flask got a problem with dissolvation: I had to add 9 gr of IPA to solve it completely. IPA weight was adjusted at the point of complete dissolvation in order to replenish the evaporated.
Also, as crystallization run, chloride flakes were seen floating on the surface in second flask. That wasn't noticed in first. Obviously density is different due to contaminants.
I had two batches, one after ABE, pure white, another one brownish after crystallization in water.
Both batches were solved by weight in IPA from the same bottle under T=65C.
Chloride weight - 70 gr
IPA weight - 193 gr
First flask dissolved completely.
Second flask got a problem with dissolvation: I had to add 9 gr of IPA to solve it completely. IPA weight was adjusted at the point of complete dissolvation in order to replenish the evaporated.
Also, as crystallization run, chloride flakes were seen floating on the surface in second flask. That wasn't noticed in first. Obviously density is different due to contaminants.
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