Synthèse de méthamphétamine à partir de P2P via Al/Hg

[Pinkbay]

Sir, can I use 35% methylamine in methanol instead of methylamine in water?

 

[Speedfac]

yes , Methylamine in Methanol its 33%.

 

[Pinkbay]

thx a lot, sir.

 

[Manisj@1290]

You have mentioned about oxidation here,
it takes me almost 7-8 hours to filter the mixture,
Because when I use vacuum, vacuum filtration cannot happen because of the aluminum amalgam sludge,
That's why I first pick up the aluminium dust through a cloth, due to which a lot of the aluminium dust comes out with the liquid, then I filter the filtrate through filter paper, which takes a lot of time
Will taking too long for filtration lead to meth base oxidation,
I also smell a lot of methylamine gas during filtration,
what effect will this have, can the meth base get spoiled due to oxidation,
how much effect will this have, please share your opinion

 

[lalalander]

Instead of being oxidized by oxygen, the methamphetamine free base forms the methamphetamine carbonate salt with carbon dioxide in the air.

 

[Manisj@1290]

I am making p2p by ethyl 2 chloropriponate method, and I have purchased methylamine solution 40%, after that I am doing the whole synthesis process step by step as shown in the video, only filtration is taking me a lot of time, but I am not able to understand whether I am getting methamphetamine free base or not, because after evaporating the dcm very little amount of oil is remaining, after introducing it again through hcl gas I am not getting the salt

 

[lalalander]

Why don't you just use NaBH4? Also you can get a yield around 85% of the glycidate you get with Ethyl-2-Chloropriponate by adding aqueous Oxone solution to a-Methyl Cinnamic Acid in acetone and NaHCO3.

Benzaldehyde + MEK = 3-methyl-4-phenyl-3-buten-2-one

3-methyl-4-phenyl-3-buten-2-one + NaClO = a-Methyl Cinnamic Acid

a-Methyl Cinnamic Acid + Oxone in NaHCO3 buffered Acetone = BMK Glycidic Acid

BMK Glycidic Acid + NaOH = BMK 5449

 

[Arakava]

Sir! What was the synthesis temperature? Did you do it in ice bath?

 

[Arakava]

I made p2p by bromine and benzen. And made 40% aqueous methylamine.
Then synthesis it by Al/hg. After filtering the aluminium amalgam. I did a steam purification. And seperated fb from ethanol and water by dcm. Then evaporated the dcm.
What's left was a pale yellow oil.
How can I make sure it's free base racemic meth?
It smells like methylamine but not that strong. I mixed it with diethyl ether then introduced hcl gas to it. It didn't give me any salt. I evaporated the diethyl ether. Some salt appeared. But smoking it had no effect.

 

[GhostChemist]

You couldn't synthesize p2p by using only bromine and benzen

 

[Arakava]

First I synthesis bromoacetone. Then synthesised penylaceton by bromoacetone and benzene in the presence of alcl3 as catalyst

 

[GhostChemist]

"How can I make sure it's free base racemic meth?" use Simin`s test or standard test-strips
http://bbzzzsvqcrqtki6umym6itiixfhn...ephedrine-hypophosphorous-acid-synthesis.111/ testing is show in the end of video