2C-feniletilamīnu sintēze

NarwhalFucker419

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Vai kādam ir informācija par 2C-H bromēšanu ar n-bromosukcinimīdu? Esmu redzējis, ka daži cilvēki to pieminēja citur, bet neesmu atradis nevienu aprakstu.
 

Raxmil

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Arī es to meklēju, bet nevarēju atrast detalizētu informāciju
Zinu tikai to, ka to var darīt GAA vai DCM, bet nav priekšstata par attiecībām.
 

amieri

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There's a person in maybe theehive on Reddit.i believe the also have a mescaline synth posted too and a few others.
 

btcboss2022

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Man ir šaubas par 2CB sintēzes pēdējo soli. Tur ir teikts: "Reakcijas maisījumam ļāva atgriezties istabas temperatūrā, filtrēja un cietās vielas saudzīgi izskaloja ar aukstu etiķskābi." Kamēr es zinu, ka etiķskābe kļūst cieta 16-17C temperatūrā, tad ko tieši nozīmē auksta etiķskābe?
Paldies.
 

G.Patton

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Sveiki. es pieņemu, ka aukstā skābe nozīmē istabas temperatūrā, jo ir paskaidrojums, ka reakcijas laikā izdalās siltums.
 
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btcboss2022

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Ok ok, es arī tā domāju, bet es gribēju apstiprināt, jo jūs zināt, kad mēs sakām auksts parasti mēs domājam no saldētavas nevis RT hahaha, bet ar etiķskābi tas nav iespējams ;-) paldies.
 

w2x3f5

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Es īsti nesaprotu, kāpēc mazgā amīna hidrobromīdu, to nav iespējams lietot, tas deg. Labāk ir attīrīt un iegūt hidrohlorīdu, un zaudējumi ir mazāki, kā arī izvairīties no apšaubāmiem mēģinājumiem izmazgāt pulveri no broma.
 

nujrc

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Es saprotu, ka atlikušais elementārais broms no produkta, tāpat kā jebkurš šķīdinātājs, iztvaikos gaisā, tāpēc ar laiku nepaliks saprātīgs daudzums. HCL izgatavošana bez HBr žāvēšanas - veiksmes, lai iegūtu tīrāku produktu, jo var nākties saskarties ar broma sāļiem broma/GAA šķīdumā un pašu bromu.
 

w2x3f5

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Es neredzu nekādas problēmas broma atliekas pārspēt ar tiosulfātu, pēc tam ph novest līdz sārmainai videi un savākt eļļu ar šķīdinātāju.
 

situ1984

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(R)-(+)-α-metilbenzilamīns CAS numurs:
3886-69-9 Vai tas ir no plaušām? Vai tas uzsūcas no kuņģa? Vai to var lietot tieši?
(R)-(+)-α-metilbenzilamīns CAS numurs:
3886-69-9 Vai tas nāk no plaušām? Vai to absorbē kuņģis? Vai to var lietot tieši?
 

G.Patton

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Tam nav psiholoģiskas iedarbības.
 

amieri

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Kur var iegādāties 2,5 dimetilnitrostirēnu
 

HerrHaber

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Henrija 2,5-dimetoksibenzaldehīda kondensācija ar nitrometānu primārā amīna kā katalizatora klātbūtnē.
 

amieri

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It blows my mind how far I've come in this since I wrote this . You guys are all works of inspiration thanks for sharing
 

taricshop

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Vai ir iespējams 2cb sintēzē elementāro bromu aizstāt ar hbr skābi?
@G.Patton
 

Newbee

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@HEISENBERG @WillD @G.Patton
Question to you guys.Is it possible to perform bromination of 2ch to 2cb by NBS (N-Bromosuccinimide)
instead of elemental bromine (br2)
 
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amieri

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That's seems to be the new go to I see alot.i need to get some succinimide acid n give it a try.
 

Newbee

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i found some writeups on thehivee but im not sure about it i also cant try do it on my own. but NBS seems to be safer to use than BR
 

amieri

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I use a 2×2×4 grow tent in its side with a 8" inline fan going out the building as a hood up on a folding table definitely does the job,still wear a mask non the less. Make sure you have a 5% sodium thiosulphate solution on hand in case of a accident and a rubber made bin with enough of that solution to run through you glass at the end.and think every step out. You got this my friend can't wait to hear of your success.
 

amieri

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Sure you can, obviously dig as deep as you can researching hand but the fact you came this far says a lot.so keep pushing and if you waste something you at least gain the experience.now safety if thats what your concerned about thats a horse of a different color
 
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