Hey there, first time poster long time reader of the forums here and many other chemistry groups.
Firstly, much respect to the Experts here for helping out a community of aspiring chemists, you have given me faith and much more hope on my journey of learning, and once I have gained more knowledge with organic chemistry I hope to be able to give back in some way in the near future..
Anyway to the point of my post. I've recently been learning alot on the clear-net from Rhodium and erowid archives etc to expand my scope and understanding of common techniques used in chemistry in general and I do strongly believe I am slowly getting a good grasp on all the basics so to speak. However I guess you could say I've hit a brick wall and need some advice.
Initially my hope was to learn to produce Phenyl-2-propanone (P2P), then proceed to make Crystal Meth which I have used in the past.
However, without the proper equipment at the moment (
Will soon be buying a distillation kit, proper glassware kit, Magnetic stirrer and Vaccum etc..) I honestly lost faith and became too discouraged in making any decent attempt.
I found a good source for obtaining Nitro-ethane for one of the synth's I was considering seriously through eBay, as a liquid form of 'Nail Brush Saver' along with other regeants but I still was hesitant in my ability without the equipment at hand currently.
So in the Meantime after this initial downfall I've been trying to keep positive and just soaking in as much as I can about Organic Chemistry..
Anyway, I then happened to stumble across this site reading about it on other forums and found this amazing place where the content in much more fresh and the community seems alot more educated than others I've seen and then I found this specific thread in particular which caught my attention. I really love the way the video was put together and have now shifted my focus to producing 4-MMC for the end product of my first legit experiment.
I'll soon have all of the equipment necessary to give it a real go and was hoping if I could request a couple of things without asking too much at the same time.
I've found access to all the ingredients except for a couple of obvious ones as I believe they are quite tightly controlled generally as far as I'm aware.
The regeants I'm talking about are 4-methylpropiophenone and Methylamine Hydrochloride (40% Aqueous Solution).
I have read both of links I've attached below regarding production from scratch. However, I was wondering firstly with the Methylamine, is there a way to scale the whole recipe down while still using that exact same video method in the thread there. It would really help me by making my first attempts more affordable as a whole. Or is the a smaller scale method on here you could point me to that would also be great =)
Methylamine Hydrochloride-synthesis-large-scale
In regards to scale size the proposed method below I found for 4-methylpropiophenone is workable for me, however at this stage I was hoping an expert here could possibly (pretty please) do an in depth video, or point me in the right direction for a good method that is a little more 'amateur chemist' friendly lol?
Synthesis-of-4-methylpropiophenone-from-toluene-by-friedel-crafts-reaction-1kg-scale
Thanks for your time guys and girls, and I hope to keep you all updated on my journeys and trail runs in the near future. I'm very dedicated to learning as much as possible and any help is much appreciated. Please PM me if you feel more comfortable in discussing things that way.
Cheers,
Sitr1x.