Amphetamine synthesis from P2NP via Al/Hg (video)
- Thread starter HIGGS BOSSON
- Start date
What do you mean exactly, how it was used in the preperation?
You can see the supplier list here: http://bbzzzsvqcrqtki6umym6itiixfhni37ybtt7mkbjyxn2pgllzxf2qgyd.onion/resources/
You'll create a solution of P2NP, Isopropyl Alcohol and Acetic Acid (10 g of 1-phenyl-2-nitropropene in 100 ml of isopropyl alcohol and 50 ml of acetic acid).
It is a basic mixture of the 3 above described precursors, simply mix them together!
Do you got any more questions?
Some please correct me if I'm wrong!
Cincerly,
Koko
I got some questions:
1. How can I clean the base solution from Isopropyl and other unwated byproducts so that I receive a pure amphetamine freebase?
I am looking into this synthesis to produce amphetamine freebase, not sulphate and am wondering if it is necessary to clean the spereated top layer to make it ready as pure amphetamine freebase.
2. What type of exhaust system is recommended for this reaction in a home lab?
I was reading in the thread that describes exhaust systems but am looking to find less space consuming options
3. What is the estimated yield of pure amphetamine freebase from this reaction (10g P2NP)?
I'd estimate it to be somewhat around 50ml, if the Isopropyl is fully removed from the base that's seperated
@HIGGS BOSSON
@G.Patton
@William Dampier
Evaporate solvent and you can carry out steam distillation to purify free base.
There are nice guides.
Depends on your skill, 70-90%. From 6.19 to 8 mL of amph free base. I don't know how did you calculated 50 mL
There are nice guides.
Depends on your skill, 70-90%. From 6.19 to 8 mL of amph free base. I don't know how did you calculated 50 mL
Thanks!
Thanks!
Okay, that's a surprise!
According to my sourcing costs the cost for 1.000ml of freebase should then be between 379,36€ and 546,64€, according to my research that seems a little high.
Is there a method than can reduce the production costs?
I am wondering as I am looking into the manufacturing of freebase for commercial use of freebase, so I am having the trouble to scale this reaction towards something like 2.5kg P2NP or even higher otherwise it wouldn't make much sense
What other reactions could you recommend for commercial use? I can't do this reaction 140 times to get 1L haha
I know that 1g of pure amph sulfate has aproximately cost from 20 to 30 eur. You can get ~1450g of sulphate salt from 1L of base. 546 eur looks not so bad. You have to carry out synthesis. If you have no experience, it is hard to calculate and build global plans.
One-pot synthesis of amphetamine from P2NP with NaBH4/CuCl2 (1kg scale)
One-pot synthesis of amphetamine from P2NP with NaBH4/CuCl2 (1kg scale)
I just want to find the most efficient (time and money) method to be able to know what to focus on.
20 - 30 EUR sounds like a dream haha, where I'm from we sell a kilo of Speed for 800€ - 1.000€
Thanks, I've read into that already but it seems very costy, as far as I understood this method has around 2.5x the price of the Synthesis via Al/Hg & P2NP
Basically for both..the people don't really care if there's coffeine cut into it or not..which is sad
Deff. not red/brown.Red brown organic layer means overheating if the coloration appeared before basification, if it's after it's your p2np and other side products moving with the ipa to the organic layer because of uncomplete reaction (in this case it should be yellowish brown, not so intense redish brown)
Is there anyone that has experience with scaling this reaction to 2.5kg+ P2NP who would be willing to answer some questions?