JWH-018 synthesis. Small scale.
- Thread starter WillD
- Start date
out of researches, i know now here it is like this: when recieve a package from abroad, it must have an invoice in spanish, and every post office has an own customs department inside. Packages arrive not at your house they arrive at the post office. you have to be registered there, with phone number and they message you if something arrives. then you have to go there and open it with them together. It was even not easy to find such information.
is it in mexico easy to get the required stuff imported? or maybe in guatemala if someone knows?
There is manual, what exactly don't you understand?
I don't understand your question. There is two different steps: step 1 with Al2O3 and step 6 with reflux. You have to just repeat manual.
What did you do exactly? Can you explain your procedure step-by-step?
I don't understand your question. There is two different steps: step 1 with Al2O3 and step 6 with reflux. You have to just repeat manual.
What did you do exactly? Can you explain your procedure step-by-step?
In step 4, are the sodium and bromopentane mixed in first, or are they mixed into the mixture one by one?
And the step 7, what does it mean that the aluminum oxide is filtered first? Is aluminum mixed into mixtured first or what?
And also during the reflux process, what temperature should we use?
Please explain in more detail step 8.
Help.
And the step 7, what does it mean that the aluminum oxide is filtered first? Is aluminum mixed into mixtured first or what?
And also during the reflux process, what temperature should we use?
Please explain in more detail step 8.
Help.
The sequence is described in step 4. Do it one by one.
What don't you understand? Read about gravity filtration here.
Add 10 ml of water to the reaction vial, place reaction mixture into a freezer and crystalline JWH-018 is formed. Product is filtered on a Schott funnel and Buchner flask.
Suction (vacuum) filtration
You have to click links and read by yourself. Lab FAQ section consist of wide detailed explanations for all necessary procedures.
What don't you understand? Read about gravity filtration here.
Add 10 ml of water to the reaction vial, place reaction mixture into a freezer and crystalline JWH-018 is formed. Product is filtered on a Schott funnel and Buchner flask.
Suction (vacuum) filtration
You have to click links and read by yourself. Lab FAQ section consist of wide detailed explanations for all necessary procedures.
Temperature of reflux means temperature when the solution is boiled. You can check solvent boiling point. Do you understand?
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