Sinteza metamfetamina iz P2P z redukcijo z NaBH4. Srednja stopnja.

btcboss2022

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Naredil sem novo serijo s 14 moli in to je dobljeni izkoristek:
1932gr "umazanega" P2P = 1600ml olja brez meth-baze
Olje bom odtehtal, da bodo številke pravilne, se opravičujem ;-)
 

G.Patton

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Ali znate pisati v odstotkih? %
 

btcboss2022

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Tehtam ga 1340gr metinega olja je približno 70 % Mislim, da ga lahko vseeno izboljšam.
 

G.Patton

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1340 g brez metamfetaminske baze iz 1932 g p2p je 62,4 %. Kakor koli že, čestitke!
 

btcboss2022

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Pozdravljeni,

ta postopek sem uporabil z MDP2P namesto P2P, da bi imel olje brez MDMA, in deluje, kot si predstavljam.
Upoštevajte molsko maso MDP2P, ostalo je popolnoma enako.
 

Bartholomeus

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Koliko gramov MDP2P ste uporabili?
Kolikšen je bil izkoristek?
In ali ste uporabili ''umazano'' olje pmk neposredno iz pretvorbe voska pmk?
 

btcboss2022

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Vsak mol MDP2P je 178 g
Uporabil sem "umazano" pmk ja, naslednjo serijo bom upošteval izkoristke.
 

callmecharlie

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vau, to je odlična stvar! Hvala za dokumentiranje postopka
 

BongMan

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Ali lahko dimimo sulfatno sol? poskusil sem in sulfatna sol je zelo enostavna za izdelavo, samo dodajte H2SO4 10 % in mešanico acetona ter filtrirajte oborino, sperite z acetonom, da jo očistite ...
 

Ortist

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ne sulfatov ni mogoče kaditi. razgradi se pred izhlapevanjem
 

G.Patton

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Verjetno da, vendar je vohljanje bolj pogosta in ustrezna metoda
 

Mr.Blanks00

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Mi
pri tej metodi uporabljate metilamin hcl ali prosto bazo?
Ali pri tej metodi uporabljate metilamin hcl ali freebazo?
 
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Mr.Blanks00

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Ali pri tej metodi uporabljate metilamin hcl ali prosto bazo?
 

G.Patton

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Pozdravljeni, v svoji objavi morate uporabljati samo angleški jezik, nadaljnje objave v drugih jezikih bodo izbrisane. Drugi jeziki so na voljo v zasebnih sporočilih in lokalnih skupinah.
Brezplačna podlaga. V tej publikaciji nisem omenil oblike soli.
 

callmecharlie

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G Pattons v začetni objavi uporablja freebase, vendar mislim, da če ste se v komentarjih nanašali na objavo btcboss2022, je uporabil trdni metilamin hcl, ki ga je raztopil v metanolu. To je moja razlaga. Upam, da to pomaga

 

Mr.Blanks00

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No, hvala za informacije, ja, nanašam se na komentar btcbossa, ker ga je napisal z metilaminom hcl, zato sem vprašal agr ni zmeden.
 

callmecharlie

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da, mislim, da je to ena od "različic" iste metode, ki jih omenja. Hs je opravil izvrstno delo.
 

triwps369

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Ali je potrebno ločevanje izomerov D in L?
Ali ne morem preprosto kristalizirati olja brez ločevanja izomerov?
 

G.Patton

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Pozdravljeni, da. Lahko brez težav. Upoštevajte, da iz racemične zmesi ne bi mogli pridelati velikih drobcev.
 

triwps369

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Ali bodo črepinje majhne ali bo to prah?
 
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