Sinteza amfetamina iz P2NP prek SnCl2 in Zn

TucoSalamanca.

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kaj lahko uporabimo namesto magnezijevega sulfata
 

mithyl2

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Magnezijev sulfat je po mojem mnenju zelo lahko dobiti po vsem svetu. Imate težave pri njegovem pridobivanju?

in ga morate pred uporabo popolnoma posušiti. Jaz sem ga dal v mikrovalovno pečico.
 

GDC

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Enak problem je tudi tukaj...
Po cinku in hidroksidaciji rumena snov na vrhu in po dodajanju DCM:
Na vrhu je čista raztopina (PH7 na lestvici 14), na dnu pa mlečna snov (PH 11)...
Toda na tvojih fotografijah je drugače.

Katero pot ste uporabili? Propen do oksima s SnCl2/HCl in nato?

Lep pozdrav
 
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GDC

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Nisem prepričan o času... GAA -> cink -> NaOH ?? Max. Temperatura ???

KorakOpremaKemikalije
1. PRIPRAVA;čaša 100 ml15 g P2NP; 50 ml acetona
2. PRIPRAVA;čaša 500mlRaztopina NaOH, H2O 1:1 (200g;200ml)
3. PRIPRAVA: NAHAOH (2) 3;čaša 150mlRaztopina NaOH, H2O 1:2 (50g;100ml)
4. PRIPRAVA: NAHAOH (2,5 ML); 2;erlenmajerica 250ml, temperaturni senzor, povratni kondenzator50 ml acetona; 42 g SnCl2; raztopina P2NP;
5. DODAJTE;50 ml acetona; 42 g SnCl2;
6. ADD;Raztopina P2NP;
7. DELO; 20 min.Mešalnik
8. PRIPRAVA;čaša 150 ml;Raztopina HCl (150 ml H2O; 4 ml HCl);)
9. DODAJ; v čašoraztopina HCl
10. PRIPRAVI;čašo 1000 ml
11. DODAJTE;Mešanico prenesite v čašo
12. DODAJ;400 ml pripravljene raztopine NaOH v razmerju 1:1; !PH11!
13. PRIPRAVI;500ml čaša, Buchnerjeva čaša, Erlenmeyerjeva čaša, brizgaEtil acetat, MgSO4
14. EKSTRAKT;mešalnik, brizga3x50ml etil acetata
15. SUŠENJE;MgSO4
16. FILTRIRAJTE;Erlenmeyer, Buchner
17. PRIPRAVI;500ml bučka, mešalnik60 ml GAA, 10 g cinka
18. DODAJTE;60 ml GAA
19. DODAJ;Mešanica oksima
20. ADD;10 g cinka
21. DELO; 15 min.Mešalnik
22. PRIPRAVABuchner, Erlenmeyer
22. DODAJTE;150 ml pripravljene raztopine NaOH v razmerju 1:2; !PH11!
23. FILTRIRAJTE;Erlenmeyer, Buchner
24. PRIPRAVI;500ml čaša, Buchner, Erlenmeyer50 ml DCM
25. DODAJTE;filtrirana mešanica
26. DODAJ;50 ml DCM
27. PRIPRAVI;100ml čaša, brizgaMgSO4
28. LOČITE;Sloj DCM je spodnji sloj.
29. SUŠIMO;MgSO4
30. FILTRIRAJTE;Erlenmeyer, Buchner
31. PRIPRAVI;250ml čaša, Buchner, Erlenmeyer50 ml acetona; želena kislina
32. DODAJTE;filtrirano organsko plast
33. ADD;50 ml acetona
34. DODAJTE: 1;želena kislina
29. OHLADITE;Zamrzovalnik
35. FILTRAT;Erlenmeyer, Buchner
220 min.
 
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GDC

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Ali boste to dodali kot en del ali počasi = kako dolgo? Reagira zelo eksotermno
 

TucoSalamanca.

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Iz 15 gramov p2np sem dobil 5 gramov amfetamina.


ZauN1EcjsM
 
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GDC

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Koliko časa potrebujete za del s cinkom? (H2 Generation)
 

TucoSalamanca.

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Kako posušiti izdelek po filtraciji Nimam kompleta za vakuumsko filtracijo
 

GDC

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Filtriranje s kavnim filtrom in acetonom + pustite, da se posuši na zraku.
 
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GDC

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~5-10 ml na g
 

GDC

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in malo premešajte, vendar previdno ... druga rešitev je stara kavbojka in jo stisnite
 

GDC

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Kako dolgo je trajalo ustvarjanje H2 s cinkom? (Dokler ni bila pripravljena aminska baza)
 
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GDC

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Ali ste ohladili mešanico?
Ali ste dodali ves NaOH? Počasi ali hitro? (v obeh primerih)
Kakšna je bila najvišja temperatura med dodajanjem?
 

TucoSalamanca.

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Mešanice nisem ohladil
Da, v fazi 2 je reakcija res eksotermna. Dodajal sem jo počasi.
 
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TucoSalamanca.

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Če želite izdelati alkalijo, namesto natrijevega hidroksida uporabite natrijev karbonat. Morda bo vaša težava rešena. Uporabljam natrijev karbonat.
 
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pingu

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Ali lahko objavite seznam sestavin?
 

GDC

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Mislim, da je odsoten
 

GDC

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1-fenil-2-nitropropen
15
g
Aceton
50
ml
Sn(II)Cl * 2H2O
42
g
Aceton
50
ml
HCl
4
ml
Voda
150
ml
NaOH
200
g
Voda
200
ml
Etil acetat
150
ml
MgSO420 % prostornine končne raztopine
OCETNA KISLINA (GAA)
60
ml
Cink
10
g
NaOH
50
g
H2O
100
ml
DCM
110
ml
MgSO420 % prostornine končne raztopine
Aceton
50
ml
 
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