Sinteza amfetamina iz P2NP prek SnCl2 in Zn

TucoSalamanca.

Don't buy from me
Resident
Language
🇹🇷
Joined
May 7, 2023
Messages
201
Reaction score
27
Points
28
kaj lahko uporabimo namesto magnezijevega sulfata
 

mithyl2

Don't buy from me
Resident
Language
🇬🇧
Joined
Aug 19, 2022
Messages
264
Reaction score
27
Points
28
Magnezijev sulfat je po mojem mnenju zelo lahko dobiti po vsem svetu. Imate težave pri njegovem pridobivanju?

in ga morate pred uporabo popolnoma posušiti. Jaz sem ga dal v mikrovalovno pečico.
 

GDC

Don't buy from me
Resident
Language
🇬🇧
Joined
Apr 30, 2022
Messages
42
Reaction score
10
Points
8
Enak problem je tudi tukaj...
Po cinku in hidroksidaciji rumena snov na vrhu in po dodajanju DCM:
Na vrhu je čista raztopina (PH7 na lestvici 14), na dnu pa mlečna snov (PH 11)...
Toda na tvojih fotografijah je drugače.

Katero pot ste uporabili? Propen do oksima s SnCl2/HCl in nato?

Lep pozdrav
 
Last edited:

GDC

Don't buy from me
Resident
Language
🇬🇧
Joined
Apr 30, 2022
Messages
42
Reaction score
10
Points
8
Nisem prepričan o času... GAA -> cink -> NaOH ?? Max. Temperatura ???

KorakOpremaKemikalije
1. PRIPRAVA;čaša 100 ml15 g P2NP; 50 ml acetona
2. PRIPRAVA;čaša 500mlRaztopina NaOH, H2O 1:1 (200g;200ml)
3. PRIPRAVA: NAHAOH (2) 3;čaša 150mlRaztopina NaOH, H2O 1:2 (50g;100ml)
4. PRIPRAVA: NAHAOH (2,5 ML); 2;erlenmajerica 250ml, temperaturni senzor, povratni kondenzator50 ml acetona; 42 g SnCl2; raztopina P2NP;
5. DODAJTE;50 ml acetona; 42 g SnCl2;
6. ADD;Raztopina P2NP;
7. DELO; 20 min.Mešalnik
8. PRIPRAVA;čaša 150 ml;Raztopina HCl (150 ml H2O; 4 ml HCl);)
9. DODAJ; v čašoraztopina HCl
10. PRIPRAVI;čašo 1000 ml
11. DODAJTE;Mešanico prenesite v čašo
12. DODAJ;400 ml pripravljene raztopine NaOH v razmerju 1:1; !PH11!
13. PRIPRAVI;500ml čaša, Buchnerjeva čaša, Erlenmeyerjeva čaša, brizgaEtil acetat, MgSO4
14. EKSTRAKT;mešalnik, brizga3x50ml etil acetata
15. SUŠENJE;MgSO4
16. FILTRIRAJTE;Erlenmeyer, Buchner
17. PRIPRAVI;500ml bučka, mešalnik60 ml GAA, 10 g cinka
18. DODAJTE;60 ml GAA
19. DODAJ;Mešanica oksima
20. ADD;10 g cinka
21. DELO; 15 min.Mešalnik
22. PRIPRAVABuchner, Erlenmeyer
22. DODAJTE;150 ml pripravljene raztopine NaOH v razmerju 1:2; !PH11!
23. FILTRIRAJTE;Erlenmeyer, Buchner
24. PRIPRAVI;500ml čaša, Buchner, Erlenmeyer50 ml DCM
25. DODAJTE;filtrirana mešanica
26. DODAJ;50 ml DCM
27. PRIPRAVI;100ml čaša, brizgaMgSO4
28. LOČITE;Sloj DCM je spodnji sloj.
29. SUŠIMO;MgSO4
30. FILTRIRAJTE;Erlenmeyer, Buchner
31. PRIPRAVI;250ml čaša, Buchner, Erlenmeyer50 ml acetona; želena kislina
32. DODAJTE;filtrirano organsko plast
33. ADD;50 ml acetona
34. DODAJTE: 1;želena kislina
29. OHLADITE;Zamrzovalnik
35. FILTRAT;Erlenmeyer, Buchner
220 min.
 
Last edited:

GDC

Don't buy from me
Resident
Language
🇬🇧
Joined
Apr 30, 2022
Messages
42
Reaction score
10
Points
8
Ali boste to dodali kot en del ali počasi = kako dolgo? Reagira zelo eksotermno
 

TucoSalamanca.

Don't buy from me
Resident
Language
🇹🇷
Joined
May 7, 2023
Messages
201
Reaction score
27
Points
28

Iz 15 gramov p2np sem dobil 5 gramov amfetamina.


ZauN1EcjsM
 
  • Like
Reactions: GDC

GDC

Don't buy from me
Resident
Language
🇬🇧
Joined
Apr 30, 2022
Messages
42
Reaction score
10
Points
8
Koliko časa potrebujete za del s cinkom? (H2 Generation)
 

TucoSalamanca.

Don't buy from me
Resident
Language
🇹🇷
Joined
May 7, 2023
Messages
201
Reaction score
27
Points
28
Kako posušiti izdelek po filtraciji Nimam kompleta za vakuumsko filtracijo
 

GDC

Don't buy from me
Resident
Language
🇬🇧
Joined
Apr 30, 2022
Messages
42
Reaction score
10
Points
8
Filtriranje s kavnim filtrom in acetonom + pustite, da se posuši na zraku.
 
View previous replies…

GDC

Don't buy from me
Resident
Language
🇬🇧
Joined
Apr 30, 2022
Messages
42
Reaction score
10
Points
8
~5-10 ml na g
 

GDC

Don't buy from me
Resident
Language
🇬🇧
Joined
Apr 30, 2022
Messages
42
Reaction score
10
Points
8
in malo premešajte, vendar previdno ... druga rešitev je stara kavbojka in jo stisnite
 

GDC

Don't buy from me
Resident
Language
🇬🇧
Joined
Apr 30, 2022
Messages
42
Reaction score
10
Points
8
Kako dolgo je trajalo ustvarjanje H2 s cinkom? (Dokler ni bila pripravljena aminska baza)
 
View previous replies…

GDC

Don't buy from me
Resident
Language
🇬🇧
Joined
Apr 30, 2022
Messages
42
Reaction score
10
Points
8
Ali ste ohladili mešanico?
Ali ste dodali ves NaOH? Počasi ali hitro? (v obeh primerih)
Kakšna je bila najvišja temperatura med dodajanjem?
 

TucoSalamanca.

Don't buy from me
Resident
Language
🇹🇷
Joined
May 7, 2023
Messages
201
Reaction score
27
Points
28
Mešanice nisem ohladil
Da, v fazi 2 je reakcija res eksotermna. Dodajal sem jo počasi.
 
  • Like
Reactions: GDC

TucoSalamanca.

Don't buy from me
Resident
Language
🇹🇷
Joined
May 7, 2023
Messages
201
Reaction score
27
Points
28
Če želite izdelati alkalijo, namesto natrijevega hidroksida uporabite natrijev karbonat. Morda bo vaša težava rešena. Uporabljam natrijev karbonat.
 
  • Like
Reactions: GDC

pingu

Don't buy from me
Resident
Language
🇳🇴
Joined
Dec 21, 2022
Messages
13
Reaction score
13
Points
3
Ali lahko objavite seznam sestavin?
 

GDC

Don't buy from me
Resident
Language
🇬🇧
Joined
Apr 30, 2022
Messages
42
Reaction score
10
Points
8
Mislim, da je odsoten
 

GDC

Don't buy from me
Resident
Language
🇬🇧
Joined
Apr 30, 2022
Messages
42
Reaction score
10
Points
8
1-fenil-2-nitropropen
15
g
Aceton
50
ml
Sn(II)Cl * 2H2O
42
g
Aceton
50
ml
HCl
4
ml
Voda
150
ml
NaOH
200
g
Voda
200
ml
Etil acetat
150
ml
MgSO420 % prostornine končne raztopine
OCETNA KISLINA (GAA)
60
ml
Cink
10
g
NaOH
50
g
H2O
100
ml
DCM
110
ml
MgSO420 % prostornine končne raztopine
Aceton
50
ml
 
Top