3-(1-Naphthoyl)indole Synthesis

[WillD]

I will write in PM about the problem in the synthesis

 

[Alex7920]

Does 3-(1-Naphthoyl)indole synthesis alone have a psychoactive effect?

 

[WillD]

There may be different reasons. When we do, we will publish it here.

 

[Eagle1234]

I have also had this problem I suspect it's due to not controlling the temperature. When do you suggest a solution to this problem?

 

[charmingcho]

thank you !

 

[madmoney69]

as we talked on private, remove insoluble when add water with ice. and then add ethyl acetate.
first time I not remove insoluble and get sticky stuff, next time I filter out and remove insoluble and add ethyl acetate and get the product like it should be.

 

[madmoney69]

actually. if you get naphtoyl indole in sticky gum form and cant evaporate last bits of EA, what really works is this.
You put all that sticky oil naphtoyl indole into water and stirr for few minutes. It gets all trapped EA out of naphtoyl indole then you filter and put to dry.
After added tail, compound very active.

 

[Hoffman]

Hello everyone... Please, I find it difficult to obtain Tin(IV) chloride, and I found that its synthesis is also difficult. I have Tin(II) chloride, so is it possible to use it? Are there other alternatives that can be used instead?

 

[G.Patton]

If you can't get other reagent, you can buy ready-made 3-(1-Naphthoyl)indole from BB Listings or anywhere else.

 

[charmingcho]

Can i see this experimental video?
I'm always fail this experimental.

 

[HIGGS BOSSON]

The video of this synthesis will be ready in 2-3 months

 

[madmoney69]

Found my naphtoyl indole photo, which I made with this synthesis

 

[BumpyJohnson]

should it be this dark ?

 

[WillD]

Insufficiently cleaned intermediate. But if you use the synthesis with sodium hydroxide, then the result can be good.

 

[pvp]

Hello brother can you pm me? Please

 

[soebunies]

does anyone know the recipe for small scale?, i need direction

 

[Alex7920]

Does 3-(1-Naphthoyl)indole synthesis alone have a psychoactive effect?

 

[tripeep]

No effect