MDMA synthesis from piperonylmethylketone (PMK/MDP2P) with formic acid

[Followme38]

Can you use standard formamide instead of nmf ?

 

[CryoThio]

It will produce MDA, not MDMA, but yes, you can. The methyl group is necessary for mdma

 

[Jasonmorales77]

Could i generate MDA with this route changing something can someone explain me how?

 

[CryoThio]

There should be some write ups on here.

Mda is produced by reacting formamide with mdp2p.

Mdma is produced by reacting n methyl formamide with mdp2p.

 

[Camilo]

Would this work for synthetizing MDA from M.Dphenylacetone?

 

[blitzen.maniax]

Just a wee word of caution if you are using the S isomer for your MDMA that if you decide to go to the MDA product instead then it's the R isomer you need for MDA and the S for MDMA . The good thing is if you plan it right there's no waste

 

[bitcoinup2020]

Hello, I'm a beginner.

I would like to ask about topic 4.
4. Concentrated hydrochloric acid (HCl 36% 30 ml) is added to this solution. Than, reaction mixture is heated at 80 °C for additional 3 h.

Can I use Hydrochloric Acid 35% instead of Hydrochloric Acid 36%?

 

[2-79-790125]

bitcoinup2020
I have never successfully made any MDMA but in my research HCl 35% vs HCl 36% has no significant difference at all for any MDMA synthesis. We are fortunate that it doesn't require that exact of tolerances. To be clear, I am a complete Rookie with limited experience and this is my opinion.

 

[ZACARIASKLK123]

7.32 g in total, added as whole in one step?
or
7.32 g of formic acid, additions divided over 7h using a drip funnel?

 

[The FALCON]

Mdp2p should be oil or powder at first ?if oil how to convert powder to oil ?

 

[The FALCON]

By what can i replace hcl gas ?

 

[hider8028]

Is MDP2P oil right? How is 9Gram?

 

[Tegridy]

how long would this process take on average?

 

[WillD]

This process can be divided into two stages (and two days) getting the result on the third day. But you can scale in quantity. We will edit the published synthesis in the future to increase productivity (using additional water in the reaction).

 

[mickael1985]

Hello
What quantities of acetone and chloridric acid should it be added to the MDMA Freebase Oil? How to extract acid and acetone then? I am not a chemist thank you for explaining to me in consequence.

 

[WillD]

5:1 acetone:aq.hcl~37% at min. After crystallizes in the freezer at least a day, if you have no experience. After filtration, leave the sediment and continue to crystallize it.

 

[ImRegistered]

Can Formic acid be substituted? Hypo phosphorus?
HCl added to N-formyl-MDMA solution, what Ph should it be?
Anyone know the yeild ?

 

[Win Win]

You write PMK means can direct use PMK powder to do?

 

[Alojz]

You can create a synthesis video of PMK and MDMA

 

[The goal]

Hello everyone ,i want to ask you about something,in mdma synthesis,what are the alternatives of di ethyl ether?can i use toluene or dcm?,also about hcl gas,can i use hcl liquid with aceton ,or sulfuric acid?also about mgso4 quantity,thanks

 

[The goal]

In number 4,how much hcl needed for 3L oil ?