MDMA synthesis via NaBH4 from MDP2P

AKWA

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Anhydrous. Or as close to
 

Studenttt

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When i have the mdma freebase i mix it 1:2 white aceton and bring ph to 2/3 and put it in freezer for 24 hours.
But nothing come? Somebody can help me?
 
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Woodshack

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Your Ratios are all wrong, You need a ph range of 7 - 6.5, because your PH is 2-3 your powder will solute again. Your next problem is that you need to make sure your Acetone is anhydrous and you need a Freebase to Acetone ratio of 1:4.
 

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I guess you overestimate MDMA FB solubility in DCM, petroleum ether, hexanne and similar solvents. In the reality it is about 3-4 ml of those solvents per 1 gr of base.
 

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Funny, but MDP2P cas 4676-39-5 and NaBH4 here are used in molar proportions 5.78 (1000 gr) : 2.56 (100 gr). Is it a mistake?
 

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@G.Patton general, is there any advantage to use Methylamine aqueous solution cas 74-89-5 against Methylamine HCl cas 593-51-1 + NaOH?
 
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G.Patton

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There is no an option to use methylamine water solution with NaBH4.
 

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If I understand it correctly, T must be kept 8-10C while all the stirring process.

What is expected ice consumption for 20-30L jacketed reactor used with a pump, submerged to a ice bath? Or this is wrong concept, and better to target for flow electric cooler?
 

G.Patton

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during NaBH4 addition, you can stir at room temp for 2 days.
Hi, I can't answer you. Depends on your addition speed and other factors.
 

alquimista00

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sodium boronhudridecanbe substituted for something different in this process that perfoms the same function.
 

Win Win

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Can change methylamine hci to solution?
 

G.Patton

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I don't understand your question.
 
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Win Win

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Your method is using methylamine gas right? But methylamine is use methylamine HCI mix with methanol right? Can use methylamine solution to replace methylamine HCI?
 

G.Patton

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Do you understand that methylamine gas is used in order to make methylamine methanol (MeOH) solution? Not methylamine hydrochloride methanol solution. You can directly use methylamine free base methanol solution.
 

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I had the same question. I have a stockpile of methylamine HCl . wondering how to use that correctly with this process.....
 
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