Čiščenje amfetamina s kislinsko-bazično ekstrakcijo

G.Patton

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Da, dobili boste amfofosfat.
 

ASheSChem

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Končno sem poskusil; vendar v moji bučki ni nobene reakcije

v moji erlenmajerici se ni pojavil noben mlečni oblak
 
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G.Patton

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Ali ste kislino dodali neposredno k amfobazi?
 

ASheSChem

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Ne, poskusil sem z mešanico acétone, kot je 10:1
 

ASheSChem

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Naslednjič bom poskusil :)
 

Berlin777

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nekoč sem poskusil to metodo, vendar se je med dodajanjem raztopine NaOH pojavila bela oborina, tako da nisem mogel presaditi
 

rabbitass

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ali se nanaša na kaj takega? faze niso bile ločene
SrUFD7xY2a
 
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Berlin777

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Ja, nekaj takega, pričakoval sem, da bom imel olje, vendar nisem videl nobenega narazen trdnih snovi
 

rabbitass

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ali se nanaša na kaj takega? faze niso bile ločene
Ali ni to amfetamin?
 

G.Patton

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Pozdravljeni, ali mi lahko, prosim, poveste, na katerem koraku točno je nastala?
 

rabbitass

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Amfetamin sem raztopil v razmerju 1 : 1 v vodi, za raztapljanje vsega sem moral dodati še malo vode. Voda je imela pH 1. Dodajal sem kapljice vode z NaOH, dokler nisem dobil pH 12. Takrat je nastala bela masa.
 

G.Patton

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To je sol primesi, ki jo ima vaš amfetamin. Sol amfetamina ne more ustvariti pH 1 v vodi. To je kislina. Po dodatku NaOH ta kislina tvori netopno sol z Na. Lahko jo filtrirate.
 

rabbitass

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Ali lahko kot topilo namesto DCM ali dietiletra uporabim toluen? Nobenega od teh dveh topil ne morem dobiti.


Olje ni nastalo, ali ste vodo filtrirali, da bi odstranili trdno snov, in nato poskušali iz vode ekstrahirati amfetamin?

Se opravičujem, da toliko sprašujem, skušam s svojimi sredstvi izvedeti vse, kar lahko, vendar so informacije omejene.
 

G.Patton

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Pozdravljeni, ni vam žal.
Da, lahko uporabite toluen.
Da, postopki so pravilni. Vendar se zdi, da amfetamina ni.
 

rabbitass

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@G.Patton Zakaj faze niso bile ločene? Videti so kot steklena vlakna, vendar olje ni bilo izdelano.
 

kitboy

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Kaj je trdna snov, ki nastane pri raztapljanju amfetamina v vodi? pri segrevanju, če se raztopi v vodi
 
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